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The vial was connected to a water condenser and refluxed for 60 min. The cooled mixture was washed with 5% sodium bicarbonate (2 x 1.0 mL). Sodium sulfate was added to the vial and the crude ester was removed and transferred to a clean vial. The vial was sealed and allowed to stand for 48 hr at rt. The clear liquid was distilled using a Hickman still and hot plate. The purified ester was removed from the still head to yield isopentyl acetate (0.29 g, 25%) and observed as a clear liquid. bp 140°C (lit1 142°C).
Discussion
The sulfuric acid catalyzed Fischer esterification of isopentyl alcohol and acetic acid provided the product isopentyl acetate in 25% yield as a clear liquid...
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