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In this experiment, 85% phosphoric acid was used as the acid catalyst. The alcohol dehydration required an acid catalyst and heat and the reaction was conducted in a simple distillation apparatus. Since, cyclohexene has a lower boiling point than cyclohexanol, cyclohexene can be distilled as it forms. So as the mixture was heated, cyclohexene distills out and is collected in a conical flask. Cyclohexanol, phosphoric acid, and water are left in the distilling flask because of their high boiling points. However, since a small amount of water may still appear after transferring the product from the conical flask, a drying agent is used to separate the cyclohexene and the remaining water is removed...
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