Title: Acetylsalicylic Acid Synthesis

Essay Details

Subject: Science
Author: Daniel Z
Date: August 15, 2015
Level: University
Grade:
Length: 3 / 654
No of views: 0
Essay rating: good 0, average 0, bad 0 (total score: 0)

Essay text:

Add .480mL of acetic anhydride and a drop of concentrated phosphoric acid. Drop in a magnetic spin vane and attach air condenser to vial. Partially submerge it in hot water. Stir with spin vane to dissolve salicylic acid. After mixture dissolves, heat for 8 to 10 minutes. Crystallize the Acetylsalicylic acid by cooling the mixture...

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Then add 3.0mL of water and stir. Set up a Hirsh funnel for vacuum filtration. Add 1mL of cold water to help transfer all of crystallized substance. Rinse crystals with water once all collected in funnel. Let crystals dry in funnel. Let finish drying on a watch glass for the week. After a week take the product, and weigh it in a pre-weighed beaker...

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